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CasNo: 220901-25-7
MF: C9H9BrO3
Disclosed is a method for producing benz...
Flash vacuum pyrolysis of ortho-methyl a...
2-methoxy-6-methyl-benzoic acid
3-bromo-6-methoxy-2-methylbenzoic acid
Conditions | Yield |
---|---|
2-methoxy-6-methyl-benzoic acid; With bromine; In chlorobenzene; at 15 ℃; for 3h;
at 35 ℃; for 2h;
|
95% |
With bromine; In acetic acid; for 2.5h;
|
70% |
3-bromo-6-methoxy-2-methylbenzoic acid
5-bromo-2-methoxy-6-methyl-benzoic acid chloride
Conditions | Yield |
---|---|
With thionyl chloride; In DMF (N,N-dimethyl-formamide); chlorobenzene; at 50 ℃; for 3h;
|
99.5% |
With thionyl chloride; N,N-dimethyl-formamide; Heating;
|
2-methoxy-6-methyl-benzoic acid
5-bromo-2-methoxy-6-methyl-benzoic acid chloride
metrafenone