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CasNo: 69260-42-0
MF: C14H16O5
PURPOSE: A photosensitive polymer prepar...
The present invention relates to a novel...
This invention provides a chemical compo...
The synthesis and phase behavior of thre...
4-(ω-hydroxybutoxy)benzoic acid
acryloyl chloride
4-[(4-propenoyloxy)butyloxy]benzoic acid
Conditions | Yield |
---|---|
With N,N-dimethyl-aniline; In N,N-dimethyl acetamide; at 0 - 20 ℃; Inert atmosphere;
|
|
With dmap; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;
|
33 g |
4-(ω-hydroxybutoxy)benzoic acid; With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;
acryloyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 25h;
|
4-(ω-hydroxybutoxy)benzoic acid
acrylic acid
4-[(4-propenoyloxy)butyloxy]benzoic acid
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid; hydroquinone; In chloroform; Dean-Stark; Reflux;
|
65% |
4-(ω-hydroxybutoxy)benzoic acid
acrylic acid
acryloyl chloride
Ethyl 4-hydroxybenzoate
2-methyl-1,4-phenylene bis(4-(4-(acryloyloxy)butoxy)-benzoate)